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Additional resources for Amino Acids in Animal Nutrition
Munoz, O. and Rastrepo J. (1999) Determination of free amino acids in raw muscle of salmon (Salm salar) by HPLC. Precolumn derivatization with phenylisothiocyanate. Alimentaria 299, 77–80. , Fuchs, D. O. (1992) Quantitative determination of amino acids from hydrolysates: evaluation of an interlaboratory test with classical ion exchange amino acid analyzers and HPLC-systems with OPA/FMOC-precolumn derivatization. Mitteilungen aus dem Gebiete der Lebensmitteluntersuchung und Hygiene 83, 457–466.
Nielsen and Hurrell (1984), having conducted comparative tests, suggested hydrolysis with sodium hydroxide in an evacuated vessel (110°C, 20 h) with the addition of 5-methyltryptophan as internal standard and hydrolysed starch. Werner (1986) and Rogers and Pesti (1990) on the other hand preferred to work with lithium hydroxide after flushing with nitrogen, without using an internal standard, because sodium hydroxide readily attacks glass, and they reported a 97–99% tryptophan recovery. Slump et al.
1999) HPLC method for analysis of free amino acids in fish using o-phthaldialdehyde precolumn derivatization. Journal of Agricultural and Food Chemistry 47, 5100–5107. D. R. (2001) Free amino acids in dark- and white-muscle fish as determinated by o-phthaldialdehyde precolumn derivatization. Journal of Food Science 66, 72–77. 12 Amino Acids in Feeds. In: Official Methods of Analysis, 16th edn. AOAC International, Arlington, Virginia, chapter 4, 4–4H. -C. and Toldra, F. (1991) Deproteinization for HPLC amino acid analysis in fresh pork muscle and dry-cured ham.